Zircon U-Pb ages and geochemical characteristics of Late Mesozoic volcanic rocks from Shibazhan-Hanjiayanzi area of Da Hinggan Mountains and their tectonic significance
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摘要:
大兴安岭十八站-韩家园地区发育晚中生代基性-中酸性火山岩。选取粗面安山岩、粗面岩、流纹岩进行年代学和岩石地球化学研究。粗面安山岩LA-ICP-MS锆石U-Pb年龄为125.2±0.9 Ma，为早白垩世火山作用的产物。岩石地球化学特征表明，中酸性火山岩属于高钾钙碱性-钾玄岩系列。岩石稀土元素总量∑REE=121.42×10-6~154.43×10-6，轻、重稀土元素分异明显（La/Yb）N=19.25~31.98，在稀土元素配分图上显示右倾型，除一个流纹岩样品具显著负Eu异常外，多数样品无明显Eu负异常（δEu=0.45~0.90）。岩石具弱富集大离子亲石元素Ba、Sr，明显亏损高场强元素Nb、Ta、Ti的特征。结合区域资料，认为十八站-韩家园地区早白垩世中酸性火山岩形成于蒙古-鄂霍茨克洋闭合机制下后碰撞伸展背景。粗面安山岩、粗面岩和流纹岩系同源岩浆部分熔融与结晶分异作用的结果，岩浆来源于受俯冲流体交代的富集岩石圈地幔。
Abstract:There exist a set of basic to intermediate-acid volcanic rocks in Shibazhan-Hanjiayuan area of Da Hinggan Mountains. In this paper, chronology and petrogeochemistry of trachyandensite, trachyte and rhyolite were discussed. LA-ICP-MS zircon U-Pb dating of trachyandensite yielded an age of 125.2±0.9Ma, revealing that it was a product of the Early Cretaceous volcanism. Geochemical characteristics suggest this set of volcanic rocks should belong to high-K calc-alkaline to shoshonite series. Volcanic rocks possess characteristics of REE composition as follows:∑REE are 121.42×10-6~154.43×10-6, the fractionation between LREE and HREE is obvious with (La/Yb)N ranging from 19.25 to 31.98, the REE patterns show rightward inclining, and most samples present a weak Eu anomaly(δEu=0.45~0.90) except one rhyolite. The trace elements geochemistry is characterized by weak enrichment of LILE (Ba, Sr), accompanied by prominent negative HFSE(Nb, Ta, Ti). Combining previous regional achievements with this study, the authors have reached the conclusion that the Early Cretaceous intermediate-acid volcanic rocks were formed in a post-collision extension environment, which was related to closure of Mongolia-Okhotsk Ocean. Trachyandensite, trachyte and rhyolite were formed by partial melting and fractional crystallization of comagma, which was derived from an enrichment of lithospheric mantle and probably experienced metasomatism of subduction fluid.
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致谢: 在成文过程中桂林理工大学覃小锋教授给与了帮助，审稿专家为本文提出了详细的修改意见，帮助作者提高了本文的论证，在此一并表示衷心的感谢。
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图 1 东北地区构造分区及大兴安岭北部地质图（a，据参考文献[2, 6]修改；b，据参考文献[10, 17]修改）
1—新生代沉积盆地；2—中生代地层；3—晚古生代地层；4—前寒武纪地层；5—燕山期花岗岩；6—印支期花岗岩；7—华力西期花岗岩；8—中生代陆相火山岩；9—地质界线；10—区域断裂；11—国界线；F1—塔源-漠河断裂；F2—得尔布干断裂；F3—头道桥-鄂伦春断裂；F4—二连-贺根山-黑河断裂；F5—嫩江断裂；F6—塔溪-林口断裂
Figure 1. Tectonic subdivision of Northeast China and geological map of North Da Hinggan Mountains
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图 2 十八站—韩家园地区火山岩显微照片
Pl—斜长石；Bt—黑云母；Hb—角闪石；Qtz—石英
Figure 2. Microphotographs of the volcanic rocks from Shibazhan-Hanjiayan area
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图 3 十八站—韩家园地区粗面安山岩锆石阴极发光（CL）照片及U-Pb年龄谐和图
Figure 3. CL images of zircons and zircon U-Pb concordia diagram of trachyandensite from Shibazhan-Hanjiayan area
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图 4 十八站—韩家园地区火山岩Harker图解
Figure 4. Harker diagrams of volcanic rocks from Shibazhan-Hanjiayan area
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图 6 十八站—韩家园地区火山岩球粒陨石标准化稀土元素配分图
（球粒陨石标准化数据据参考文献[25]）
Figure 6. Chondrite-normalized REE patterns of volcanic rocks from Shibazhan-Hanjiayan area
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图 7 十八站—韩家园地区火山岩原始地幔标准化微量元素蛛网图
（原始地幔值据参考文献[25]）
Figure 7. Primitive mantle-normalized trace elements patterns of volcanic rocks from Shibazhan-Hanjiayan area
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表 1 十八站—韩家园地区粗面安山岩锆石U-Th-Pb同位素数据及测年结果
Table 1 U-Th-Pb isotopic compositions and dating results of zircons from Shibazhan-Hanjiayan area
测点号 232Th 238U Th/U 同位素原子比率 同位素年龄/Ma 10-6 207Pb/206Pb 1σ 207Pb/235U 1σ 206Pb/238U 1σ 207Pb/206Pb 1σ 207Pb/235U 1σ 206Pb/238U 1σ TW1-01 114 139 0.82 0.0491 0.0039 0.1298 0.0101 0.0192 0.0005 152 132 124 9 122 3 TW1-02 114 121 0.94 0.0508 0.0028 0.1397 0.0075 0.0199 0.0004 231 90 133 7 127 2 TW1-03 285 243 1.17 0.0517 0.0022 0.1384 0.0057 0.0194 0.0003 273 64 132 5 124 2 TW1-04 161 147 1.10 0.0497 0.0024 0.1365 0.0064 0.0199 0.0004 181 75 130 6 127 2 TW1-05 208 189 1.10 0.0509 0.0026 0.1395 0.0069 0.0199 0.0004 235 80 133 6 127 2 TW1-06 223 180 1.24 0.0502 0.0031 0.1366 0.0084 0.0197 0.0004 204 107 130 7 126 2 TW1-07 850 416 2.04 0.0505 0.0052 0.1350 0.0137 0.0194 0.0004 219 236 129 12 124 2 TW1-08 184 176 1.05 0.0493 0.0024 0.1353 0.0064 0.0199 0.0003 164 78 129 6 127 2 TW1-09 126 123 1.02 0.0493 0.0032 0.1357 0.0086 0.0200 0.0004 162 106 129 8 127 3 TW1-10 224 191 1.17 0.0486 0.0022 0.1298 0.0057 0.0194 0.0003 126 70 124 5 124 2 TW1-11 232 202 1.15 0.0503 0.0030 0.1394 0.0081 0.0201 0.0004 207 96 132 7 128 3 TW1-12 354 222 1.60 0.0529 0.0035 0.1410 0.0091 0.0193 0.0004 324 113 134 8 123 2 TW1-13 151 151 1.00 0.0488 0.0031 0.1324 0.0081 0.0197 0.0004 137 102 126 7 126 2 TW1-14 125 125 1.00 0.0499 0.0036 0.1347 0.0096 0.0196 0.0004 190 121 128 9 125 3 TW1-15 274 281 0.97 0.0488 0.0038 0.1316 0.0102 0.0196 0.0004 136 141 126 9 125 2 TW1-16 267 193 1.38 0.0495 0.0027 0.1367 0.0073 0.0200 0.0004 173 88 130 7 128 2 TW1-17 287 205 1.40 0.0488 0.0027 0.1301 0.0070 0.0193 0.0004 140 87 124 6 123 2 TW1-18 103 107 0.96 0.0488 0.0097 0.1243 0.0243 0.0185 0.0006 140 355 119 22 118 4 TW1-19 119 81 1.46 0.0470 0.0068 0.1203 0.0172 0.0186 0.0005 50 270 115 16 118 3 TW1-20 336 218 1.54 0.0486 0.0026 0.1295 0.0069 0.0194 0.0004 126 86 124 6 124 2 TW1-21 171 157 1.09 0.0502 0.0058 0.1364 0.0157 0.0197 0.0005 204 216 130 14 126 3 TW1-22 170 158 1.08 0.0486 0.0038 0.1307 0.0100 0.0195 0.0004 129 130 125 9 124 3 TW1-23 133 147 0.90 0.0486 0.0060 0.1357 0.0167 0.0203 0.0005 126 229 129 15 129 3 TW1-24 194 207 0.94 0.0486 0.0033 0.1309 0.0087 0.0195 0.0004 129 113 125 8 125 2 TW1-25 42 60 0.70 0.0487 0.0092 0.1328 0.0248 0.0198 0.0007 133 297 127 22 126 4 
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表 2 十八站—韩家园地区火山岩主量、微量和稀土元素组成
Table 2 Major, trace and rare earth elements compositions of volcanic rocks from Shibazhan-Hanjiayan area
样品编号岩性名称 SXT1粗面安山岩 SXT24
粗面岩SXT26
流纹岩SXT11
流纹岩SXT17
流纹岩SiO2 60.53 63.66 72.22 69.4 71.69 TiO2 0.61 0.53 0.16 0.34 0.04 Al2O3 17.03 15.36 12.66 15.5 13.6 TFe2O3 4.66 4.19 0.73 2.59 0.3 FeO 1.36 1.22 0.58 1.3 0.26 CaO 4.01 1.86 2 1.75 1.08 MgO 2.06 2.39 0.52 0.81 0.24 MnO 0.07 0.07 0.01 0.05 0.01 K2O 3.64 3.7 5.03 3.64 6.15 Na2O 4.03 4.94 0.87 4.28 2.93 P2O5 0.22 0.17 0.03 0.15 0.02 烧失量 3.12 2.61 5.75 1.48 3.91 总计 101.34 100.69 100.55 101.3 100.23 Mg# 72.97 77.74 61.33 52.53 62.2 σ 3.21 3.5 1.17 2.35 2.83 DI 69.44 79.29 83.94 84.62 92.94 SI 14.57 15.92 7.26 7.21 2.5 Li 17.6 19.4 16.1 17.9 11.1 Be 1.64 1.95 1.33 2.24 1.76 Nb 8.15 7.7 8.16 26.8 32.3 Sc 8.78 7.78 1.44 3.63 13.7 Zr 158 126 107 99 199 Th 5.93 7.56 11.3 9.21 2.32 Sr 601 704 3271 657 1054 Ba 1440 1163 1517 1298 827 V 81.7 66.4 13.1 34.6 128 Co 12.7 11.6 0.26 5.17 26.8 Cr 41.5 45 7.99 38.8 151 Ni 16.1 20.3 2.48 16.4 63.8 Pb 19.6 18.6 27.3 18.8 27.5 Zn 75.2 59.3 18.7 56.2 105 W 0.432 0.423 1.01 0.564 0.242 Mo 0.952 0.409 0.29 0.857 0.924 Rb 61.8 88.7 119 99.8 36 Hf 4.35 3.77 3.28 3.45 4.76 Cs 0.538 2.05 7.66 1.94 0.455 Ga 18.7 18.8 13.6 19.7 22 U 1.46 1.45 2.86 2.17 0.59 Ta 0.59 0.546 0.636 0.824 0.371 La 35.7 30.4 34.8 36.6 33.8 Ce 62.8 54.9 53.7 65.7 63.7 Pr 7.61 5.93 5.56 7.46 8.04 Nd 27.9 21.3 18.2 26.8 32.3 Sm 4.52 3.71 2.86 3.81 5.58 Eu 1.05 0.852 0.363 0.986 1.39 Gd 3.5 2.74 1.86 2.66 3.88 Tb 0.506 0.395 0.297 0.391 0.551 Dy 2.45 1.87 1.52 1.76 2.42 Ho 0.461 0.342 0.294 0.293 0.429 Er 1.25 0.917 0.776 0.698 1.09 Tm 0.205 0.139 0.123 0.111 0.165 Yb 1.33 0.938 0.926 0.821 0.943 Lu 0.198 0.137 0.137 0.113 0.142 Y 13.2 9.08 8.44 8.28 11.5 ∑REE 149.48 124.57 121.42 148.2 154.43 δEu 0.78 0.78 0.45 0.9 0.87 (La/Yb)N 19.25 23.25 26.96 31.98 25.71 注：主量元素含量单位为%，微量和稀土元素含量为10-6
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